Tailoring flavins for visible light photocatalysis: organocatalytic [2+2] cycloadditions mediated by a flavin derivative and visible light.

نویسندگان

  • Viktor Mojr
  • Eva Svobodová
  • Karolína Straková
  • Tomáš Neveselý
  • Josef Chudoba
  • Hana Dvořáková
  • Radek Cibulka
چکیده

A new application of flavin derivatives in visible light photocatalysis was found. 1-Butyl-7,8-dimethoxy-3-methylalloxazine, when irradiated by visible light, was shown to allow an efficient cyclobutane ring formation via an intramolecular [2+2] cycloaddition of both styrene dienes, considered as electron-rich substrates, and electron-poor bis(arylenones), presumably proceeding via an energy transfer mechanism.

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Enhanced photocatalytic activity of a self-stabilized synthetic flavin anchored on a TiO2 surface

Synthetic flavin molecules were anchored on Degussa P25 titanium dioxide (TiO2). The effect of their presence on the photocatalytic (PC) activity of TiO2 was studied. Under UV light, an increase in the degradation rate of ethanol was observed. This increase was accompanied by stabilization of the anchored flavin against self-degradation. The unprecedented stabilization effect was found also in ...

متن کامل

Application of Semiconductor Photocatalysis for Effective Elimination of Organic Contaminants from Sewage

The ZnO/SiO2 semiconductor nanophotocatalysis was synthesized via sol-gel method. Also, theplatinum particles were loaded on the ZnO/SiO2 nanoparticles by photoreductive method. Thestructure of catalyst was confirmed by X-ray diffraction (XRD), scanning electron microscopy(SEM) andfourier transform infrared spectroscopy (FT-IR). The XRD patterns of ZnO particlesdisplayed the nanoparticles have ...

متن کامل

Ultrasonic-assisted Method for Preparation of Cu-doped ZnS Nanoparticles in Water as a Highly Efficient Visible Light Photocatalyst

Ultrasonic-assisted method was applied for preparation of Cu+2-doped ZnS nanoparticles (mole fractions of Cu+2 ions are 0.000, 0.015, 0.030 and 0.060) in water as a template-free and green method at 30 min. The prepared nanoparticles were investigated by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray (EDX) and UV–Vis diffuse reflectance spectra (DRS)...

متن کامل

Role of Visible Light-Activated Photocatalyst on the Reduction of Anthrax Spore-Induced Mortality in Mice

BACKGROUND Photocatalysis of titanium dioxide (TiO(2)) substrates is primarily induced by ultraviolet light irradiation. Anion-doped TiO(2) substrates were shown to exhibit photocatalytic activities under visible-light illumination, relative environmentally-friendly materials. Their anti-spore activity against Bacillus anthracis, however, remains to be investigated. We evaluated these visible-l...

متن کامل

Interaction of bacterial luciferase with 8-substituted flavin mononucleotide derivatives.

Bacterial luciferase catalyzes the emission of visible light from the reaction of reduced flavin, molecular oxygen, and an n-alkyl aldehyde. The mechanism of the reaction was probed by measuring the electronic effects of various substituents at the 8-position of the flavin ring system. Substituent effects were obtained for CH3-, Cl-, CH3O-, CH3S-, F-, and H- on the rate of formation and decay o...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

عنوان ژورنال:
  • Chemical communications

دوره 51 60  شماره 

صفحات  -

تاریخ انتشار 2015